(2-aminophenyl)diphenylphosphine sulfide

Base Information

• Chemical Name: (2-aminophenyl)diphenylphosphine sulfide
• CAS No.: 1271315-43-5
• Molecular Formula: C₂₅H₂₀NPS
• Molecular Weight: 397.48
• Mol file: 1271315-43-5.mol

Synonyms:(2-aminophenyl)diphenylphosphine sulfide

Chemical Property of (2-aminophenyl)diphenylphosphine sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-aminophenyl)diphenylphosphine sulfide

There total 3 articles about (2-aminophenyl)diphenylphosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-benzylidene-2-(diphenylphosphino)benzeneamine (154638-80-9) → (2-aminophenyl)diphenylphosphine sulfide (1271315-43-5)

Guidance literature:

With sulfur; In toluene; for 2h; Inert atmosphere; Reflux;

DOI:10.1039/c0cc03064c

Reference yield:

(2-diphenylphosphino)benzeneamine (65423-44-1) → (2-aminophenyl)diphenylphosphine sulfide (1271315-43-5)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / chloroform / 16 h / Molecular sieve; Inert atmosphere; Reflux

2: sulfur / toluene / 48 h / 20 °C / Inert atmosphere

With sulfur; trifluoroacetic acid; In chloroform; toluene;

DOI:10.1002/ejoc.201700258

Reference yield:

benzaldehyde (100-52-7) → (2-aminophenyl)diphenylphosphine sulfide (1271315-43-5)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / chloroform / 16 h / Molecular sieve; Inert atmosphere; Reflux

2: sulfur / toluene / 48 h / 20 °C / Inert atmosphere

With sulfur; trifluoroacetic acid; In chloroform; toluene;

DOI:10.1002/ejoc.201700258

upstream raw materials:

N-benzylidene-2-(diphenylphosphino)benzeneamine

(2-diphenylphosphino)benzeneamine

benzaldehyde