di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

Base Information

Chemical Name:di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane
CAS No.:190258-44-7
Molecular Formula:C₂₆H₄₂O₃Si
Molecular Weight:430.703
Hs Code.:

Synonyms:di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

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Technology Process of di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

There total 1 articles about di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 56310-18-0
di-tert-butylchlorosilane

: 190258-40-3
3-Methyl-1-phenyl-6-<(tetrahydro-2H-pyran-2-yl)oxy>-1-hexyn-3-ol

: 190258-44-7
di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

Guidance literature:: With 1H-imidazole; dmap; sodium iodide; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4020(97)00257-3

Reference yield: 68.0%

: 190258-44-7
di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

: 173728-30-8
di-tert-butyl-<1-(3-iodopropyl)-1-methyl-3-phenylprop-2-ynyloxy>silane

Guidance literature:: With iodine; 1,2-bis-(diphenylphosphino)ethane; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(97)00257-3

Reference yield:

: 190258-44-7
di-tert-butyl-{1-methyl-3-phenyl-1-[3-(tetrahydropyran-2-yloxy)propyl]prop-2-ynyloxy}silane

: 130601-96-6
(E)-1-methyl-2-phenylmethylenecyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / I₂, 1,2-bis(diphenylphosphino)ethane / CH₂Cl₂ / Ambient temperature

2: 70 percent / (Bu₃Sn)2 / benzene / 12 h / 80 °C / Irradiation

3: 73 percent / TBAF / tetrahydrofuran / 6 h / Ambient temperature

With tetrabutyl ammonium fluoride; iodine; bis(tri-n-butyltin); 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1016/S0040-4020(97)00257-3