Technology Process of C16H14N2O2S2
There total 5 articles about C16H14N2O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H14O2S;
With
potassium peroxymonosulfate;
In
tetrahydrofuran; methanol; water;
at 0 ℃;
for 18h;
ammonium thiocyanate;
In
butan-1-ol;
Reflux;
DOI:10.1016/j.bmc.2013.01.058
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phosphoric acid; trifluoroacetic anhydride / 25 °C
2.1: bromine; acetic acid / 20 °C
3.1: sodium methylate / methanol / Reflux
4.1: potassium peroxymonosulfate / methanol; tetrahydrofuran; water / 18 h / 0 °C
4.2: Reflux
With
potassium peroxymonosulfate; phosphoric acid; bromine; sodium methylate; acetic acid; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2013.01.058
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phosphoric acid; trifluoroacetic anhydride / 25 °C
2.1: bromine; acetic acid / 20 °C
3.1: sodium methylate / methanol / Reflux
4.1: potassium peroxymonosulfate / methanol; tetrahydrofuran; water / 18 h / 0 °C
4.2: Reflux
With
potassium peroxymonosulfate; phosphoric acid; bromine; sodium methylate; acetic acid; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2013.01.058