Technology Process of C26H32N6O4
There total 5 articles about C26H32N6O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; ammonium chloride;
In
N,N-dimethyl-formamide;
at 160 ℃;
for 1h;
Microwave irradiation;
DOI:10.1021/jm301059b
- Guidance literature:
-
Multi-step reaction with 7 steps
1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: lithium diisopropyl amide / tetrahydrofuran; hexane; diethyl ether / -40 - 20 °C
3: hydrazine hydrate / ethanol; water / 18 h / 50 °C
4: sodium hydride / N,N-dimethyl-formamide; acetonitrile; mineral oil / 0.33 h / 120 °C / Inert atmosphere
5: ammonium formate; palladium 10% on activated carbon / dichloromethane; methanol / 40 °C
6: sodium hydride / N,N-dimethyl-formamide; mineral oil / 120 °C / Microwave irradiation; Inert atmosphere
7: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 1 h / 160 °C / Microwave irradiation
With
sodium azide; oxalyl dichloride; palladium 10% on activated carbon; ammonium formate; sodium hydride; ammonium chloride; hydrazine hydrate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jm301059b
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium diisopropyl amide / tetrahydrofuran; hexane; diethyl ether / -40 - 20 °C
2: hydrazine hydrate / ethanol; water / 18 h / 50 °C
3: sodium hydride / N,N-dimethyl-formamide; acetonitrile; mineral oil / 0.33 h / 120 °C / Inert atmosphere
4: ammonium formate; palladium 10% on activated carbon / dichloromethane; methanol / 40 °C
5: sodium hydride / N,N-dimethyl-formamide; mineral oil / 120 °C / Microwave irradiation; Inert atmosphere
6: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 1 h / 160 °C / Microwave irradiation
With
sodium azide; palladium 10% on activated carbon; ammonium formate; sodium hydride; ammonium chloride; hydrazine hydrate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/jm301059b