ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

Base Information

Chemical Name:ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate
CAS No.:1282617-38-2
Molecular Formula:C₂₁H₂₇O₇P
Molecular Weight:422.415
Hs Code.:

Synonyms:ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

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Chemical Property of ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

Chemical Property:

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Technology Process of ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

There total 6 articles about ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 64-17-5
ethanol

: 1282618-67-0
C₁₉H₂₁O₆P

: 1282617-38-2
ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 1282617-38-2
ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 1.5 h / Industry scale

1.2: 4 - 20 °C / Industry scale

1.3: 6.5 h / pH 5 / Industry scale

2.1: caesium carbonate / dimethyl sulfoxide / 8 h / 50 - 60 °C

3.1: methanesulfonic acid / dichloromethane / -40 - 0 °C

4.1: trimethylsilyl bromide / dichloromethane / 16 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With hydrogenchloride; methanesulfonic acid; trimethylsilyl bromide; caesium carbonate; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 28636-93-3
2,6-dimethyl-4-hydroxybenzyl alcohol

: 1282617-38-2
ethyl 3-[5-(2,6-dimethyl-4-phosphonomethoxybenzyl)-2-hydroxyphenyl]propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / dimethyl sulfoxide / 8 h / 50 - 60 °C

2: methanesulfonic acid / dichloromethane / -40 - 0 °C

3: trimethylsilyl bromide / dichloromethane / 16 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With hydrogenchloride; methanesulfonic acid; trimethylsilyl bromide; caesium carbonate; In 1,4-dioxane; dichloromethane; dimethyl sulfoxide;