3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline

Base Information

• Chemical Name: 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline
• CAS No.: 68469-22-7
• Molecular Formula: C₁₆H₁₀N₆S
• Molecular Weight: 318.362

Synonyms:3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline

Chemical Property of 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline

Chemical Property:

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Technology Process of 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline

There total 4 articles about 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2,3-dichloroquinoxaline (2213-63-0) + 3-phenyl-4-amino-5-mercapto-1,2,4-triazole (22706-11-2) → 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline (68469-22-7)

Guidance literature:

With tetrabutylammomium bromide; potassium carbonate; In benzene; a) RT, 2 h, b) 60 deg C, 3 h;

Reference yield:

3-amino-2-imino-2,3-dihydrothiazolo<4,5-b>quinoxaline (62933-58-8) → 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline (68469-22-7)

Guidance literature:

Multi-step reaction with 3 steps

1: Py

2: N₂H₄*H₂O

With pyridine; hydrazine hydrate;

Reference yield:

1,2-dihydro-[1,3,4]thiadiazino[5,6-b]quinoxaline-3-thione (67726-40-3) → 3-phenyl-5H-[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazino[5,6-b]quinoxaline (68469-22-7)

Guidance literature:

Multi-step reaction with 2 steps

1: N₂H₄*H₂O

With hydrazine hydrate;

upstream raw materials:

2,3-dichloroquinoxaline

3-phenyl-4-amino-5-mercapto-1,2,4-triazole

benzoyl chloride

2-hydrazino-4(H)-1,3,4-thiadiazino<5,6-b>quinoxaline

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