benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Base Information

Chemical Name:benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate
CAS No.:1268994-64-4
Molecular Formula:C₂₁H₂₁F₁₃INO₂
Molecular Weight:693.287
Hs Code.:

Synonyms:benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Suppliers and Price of benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

There total 6 articles about benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 355-43-1
n-perfluorohexyl iodide

: 1268994-49-5
N-Cbz-3,3-dimethyl-pent-4-en-1-amine

: 1268994-76-8
C₂₁H₂₂F₁₃NO₂

: 1268994-64-4
benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Guidance literature:: With sodium dithionite; water; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2010.11.090

Reference yield:

: 63721-05-1
methyl 3,3-dimethyl-4-penteneoate

: 1268994-76-8
C₂₁H₂₂F₁₃NO₂

: 1268994-64-4
benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / 5 h / Reflux

2.1: thionyl chloride / dichloromethane / 0.5 h / Cooling with ice

2.2: 5 h / Reflux

3.1: ammonia / water / 10 h / 20 °C

4.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere; Cooling with ice

5.1: potassium carbonate / 1,4-dioxane; water / 1 h / 20 °C

6.1: sodium dithionite; water; sodium hydrogencarbonate / acetonitrile / 5 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; sodium dithionite; ammonia; water; sodium hydrogencarbonate; potassium carbonate; sodium hydroxide; In 1,4-dioxane; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2010.11.090

Reference yield:

: 7796-73-8
3,3-dimethylpent-4-enoic acid

: 1268994-76-8
C₂₁H₂₂F₁₃NO₂

: 1268994-64-4
benzyl-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-4-iodo-3,3-dimethyl-undecylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / dichloromethane / 0.5 h / Cooling with ice

1.2: 5 h / Reflux

2.1: ammonia / water / 10 h / 20 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere; Cooling with ice

4.1: potassium carbonate / 1,4-dioxane; water / 1 h / 20 °C

5.1: sodium dithionite; water; sodium hydrogencarbonate / acetonitrile / 5 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; sodium dithionite; ammonia; water; sodium hydrogencarbonate; potassium carbonate; In 1,4-dioxane; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2010.11.090