(Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione

Base Information

• Chemical Name: (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione
• CAS No.: 193686-13-4
• Molecular Formula: C₂₅H₃₀N₂O₆
• Molecular Weight: 454.523

Synonyms:(Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione

Chemical Property of (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione

Chemical Property:

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Technology Process of (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione

There total 2 articles about (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-4-(4-methoxyphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione (120040-36-0) + methyl iodide (74-88-4) → (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6,6-trimethylpiperazine-2,5-dione + (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione (193686-13-4)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMF, 0 deg C, 30 min, 2.) DMF, reflux, 3 h;

DOI:10.1248/cpb.45.1120

Reference yield:

(Z)-4-(4-methoxyphenylmethyl)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione (120040-37-1) + methyl iodide (74-88-4) → (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6,6-trimethylpiperazine-2,5-dione + (Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione (193686-13-4)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 0 deg C, 30 min, 2.) THF, reflux, 3 h;

DOI:10.1248/cpb.45.1120

Reference yield: 79.6%

(Z)-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione (193686-13-4) → (Z)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione (193686-15-6)

Guidance literature:

With sulfuric acid; In trifluoroacetic acid; for 24h; Ambient temperature;

DOI:10.1248/cpb.45.1120

upstream raw materials:

(Z)-4-(4-methoxyphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

methyl iodide

(Z)-4-(4-methoxyphenylmethyl)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Downstream raw materials:

(Z)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1,6-dimethylpiperazine-2,5-dione

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