p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Base Information

Chemical Name:p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate
CAS No.:96661-44-8
Molecular Formula:C₄₀H₄₆BrN₅O₇S
Molecular Weight:820.805
Hs Code.:

p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Synonyms:p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

There total 5 articles about p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 96661-33-5
1-<4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridyl>acetic acid

: 51727-23-2
p-bromophenacyl-6-β-<(aminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

: 96661-44-8
p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 12h;

Reference yield:

: 69-53-4,19379-33-0,33993-48-5,49841-95-4,58770-00-6
ampicillin

: 96661-44-8
p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 58.8 percent / triethylamine / CH₂Cl₂ / 4 h / 0 °C

2: 60 percent / DCC / CH₂Cl₂ / 12 h / 25 °C

With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;

Reference yield:

: 111736-36-8
C₁₄H₂₁N₂O^(1-)*Li⁽¹⁺⁾

: 96661-44-8
p-bromophenacyl-6-β-<(4-n-butyl-3-(4,4-dimethyloxazolin-2-yl)-1,4-dihydropyridylmethylcarbonylaminophenylacetyl)amino>-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 25 °C

2: 60 percent / DCC / CH₂Cl₂ / 12 h / 25 °C

With dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;