Technology Process of C24H19ClN4O
There total 5 articles about C24H19ClN4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H17ClN4O;
With
oxalyl dichloride;
In
chloroform;
at 0 ℃;
for 1h;
Reflux;
With
sodium cyanoborohydride;
In
tetrahydrofuran;
at 0 - 25 ℃;
for 24h;
DOI:10.1021/jm300831b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / 0.5 h / 150 °C / Microwave irradiation
2.1: tin(II) chloride dihdyrate / ethyl acetate / 2 h / Reflux
3.1: ethanol / 48 h / Reflux
4.1: oxalyl dichloride / chloroform / 1 h / 0 °C / Reflux
4.2: 24 h / 0 - 25 °C
With
oxalyl dichloride; tin(II) chloride dihdyrate; toluene-4-sulfonic acid;
In
ethanol; chloroform; ethyl acetate;
DOI:10.1021/jm300831b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / 0.5 h / 150 °C / Microwave irradiation
2.1: tin(II) chloride dihdyrate / ethyl acetate / 2 h / Reflux
3.1: ethanol / 48 h / Reflux
4.1: oxalyl dichloride / chloroform / 1 h / 0 °C / Reflux
4.2: 24 h / 0 - 25 °C
With
oxalyl dichloride; tin(II) chloride dihdyrate; toluene-4-sulfonic acid;
In
ethanol; chloroform; ethyl acetate;
DOI:10.1021/jm300831b