2-((4-Chlorophenyl)sulfonyl)acetohydrazide

Base Information

Chemical Name:2-((4-Chlorophenyl)sulfonyl)acetohydrazide
CAS No.:36107-11-6
Molecular Formula:C8H9 Cl N2 O3 S
Molecular Weight:248.69
Hs Code.:2928000090
DSSTox Substance ID:DTXSID60384813
Nikkaji Number:J1.451.067B
Wikidata:Q82177184
ChEMBL ID:CHEMBL1548750
Mol file:36107-11-6.mol

Synonyms:36107-11-6;2-((4-Chlorophenyl)sulfonyl)acetohydrazide;2-(4-chlorophenyl)sulfonylacetohydrazide;2-(4-chlorobenzenesulfonyl)acetohydrazide;(4-chlorobenzenesulfonyl)acetic acid hydrazide;2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide;Maybridge4_002382;MLS000859154;SCHEMBL8174639;CHEMBL1548750;DTXSID60384813;HMS1527M06;HMS2786H11;MFCD00067902;AKOS005109472;MS-7116;[(4-Chlorophenyl)sulfonyl]acetohydrazide;NCGC00176613-01;SMR000459333;2-[(4-chlorophenyl)sulfonyl]ethanohydrazide;(4-chlorophenylsulfonyl)acetic acid hydrazide;FT-0748765;2-(4-Chlorobenzene-1-sulfonyl)acetohydrazide;(4-CHLOROBENZENESULFONYL)ACETICACIDHYDRAZIDE

Suppliers and Price of 2-((4-Chlorophenyl)sulfonyl)acetohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-((4-Chlorophenyl)sulfonyl)acetohydrazide 95+%
5g
$ 746.00

Biosynth Carbosynth
2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide
25 g
$ 1060.75

Biosynth Carbosynth
2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide
10 g
$ 499.10

Biosynth Carbosynth
2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide
5 g
$ 293.55

Biosynth Carbosynth
2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide
2 g
$ 138.14

Biosynth Carbosynth
2-((4-Chlorophenyl)sulfonyl)acetyl hydrazide
1 g
$ 81.25

American Custom Chemicals Corporation
2-[(4-CHLOROPHENYL)SULFONYL]ACETOHYDRAZIDE 95.00%
5MG
$ 687.35

American Custom Chemicals Corporation
2-[(4-CHLOROPHENYL)SULFONYL]ACETOHYDRAZIDE 95.00%
10MG
$ 679.14

American Custom Chemicals Corporation
2-[(4-CHLOROPHENYL)SULFONYL]ACETOHYDRAZIDE 95.00%
1MG
$ 647.61

Total 5 raw suppliers

Chemical Property of 2-((4-Chlorophenyl)sulfonyl)acetohydrazide

Chemical Property:

Melting Point:154-155 °C(Solv: methanol (67-56-1))
Boiling Point:541.8±50.0 °C(Predicted)
PKA:10.76±0.35(Predicted)
PSA：101.13000
Density:1.469±0.06 g/cm3(Predicted)
LogP:2.72500
XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:248.0022410
Heavy Atom Count:15
Complexity:317

Purity/Quality:

97% ^*data from raw suppliers

2-((4-Chlorophenyl)sulfonyl)acetohydrazide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1S(=O)(=O)CC(=O)NN)Cl

Technology Process of 2-((4-Chlorophenyl)sulfonyl)acetohydrazide

There total 5 articles about 2-((4-Chlorophenyl)sulfonyl)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 15446-25-0
methyl 4-chlorophenylsulphinylacetate

: 36107-11-6
((4-chlorophenyl)sulfonyl)acetohydrazide

Guidance literature:: With pyridine; hydrazine hydrate; In methanol; Heating;
DOI:10.1002/jhet.5570420116

Reference yield:

: 3636-65-5
ethyl 2-((4-chlorophenyl)sulfonyl)acetate

: 36107-11-6
((4-chlorophenyl)sulfonyl)acetohydrazide

Guidance literature:: With hydrazine hydrate;
DOI:10.1021/jm00271a041

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 36107-11-6
((4-chlorophenyl)sulfonyl)acetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / Reflux

2: dihydrogen peroxide; ammonium molibdate / ethanol

3: hydrazine hydrate / methanol / Reflux

With ammonium molibdate; hydrazine hydrate; dihydrogen peroxide; potassium carbonate; In methanol; ethanol; acetonitrile;
DOI:10.1021/acs.jafc.7b06061