1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Base Information

Chemical Name:1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate
CAS No.:1442462-57-8
Molecular Formula:C₄₃H₄₁N₃O₅
Molecular Weight:679.816
Hs Code.:

Synonyms:1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Suppliers and Price of 1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

There total 6 articles about 1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1442462-56-7
1-[11-[4-(1-hydroxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime

: 75-36-5
acetyl chloride

: 1442462-57-8
1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

: 1442462-53-4
1-(4-benzo[a]carbazol-11-ylphenyl)ethanone

: 1442462-57-8
1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / dichloromethane / 2.5 h / 0 - 20 °C

2: aluminum (III) chloride / dichloromethane / 2 h / 0 °C

3: hydroxylamine hydrochloride / pyridine / 80 °C

4: triethylamine / tetrahydrofuran / 2 h / 0 °C

With aluminum (III) chloride; hydroxylamine hydrochloride; triethylamine; In tetrahydrofuran; pyridine; dichloromethane;

Reference yield:

: 1442462-54-5
1-{4-[5-(2,4,6-trimethylbenzoyl)benzo[a]carbazol-11-yl]phenyl}ethanone

: 1442462-57-8
1-[11-[4-(1-acetoxyiminoethyl)phenyl]-5-(2,4,6-trimethylbenzoyl)-11H-benzo[a]carbazol-8-yl]-3-methylbutan-1-one oxime O-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 0 °C

2: hydroxylamine hydrochloride / pyridine / 80 °C

3: triethylamine / tetrahydrofuran / 2 h / 0 °C

With aluminum (III) chloride; hydroxylamine hydrochloride; triethylamine; In tetrahydrofuran; pyridine; dichloromethane;