(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

Base Information

Chemical Name:(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate
CAS No.:958882-67-2
Molecular Formula:C₁₈H₃₁NO₆SSi
Molecular Weight:417.599
Hs Code.:

Synonyms:(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

Chemical Property:

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Technology Process of (R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

There total 2 articles about (R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₁₁H₂₅NO₄Si

: 98-59-9
p-toluenesulfonyl chloride

: 958882-67-2
(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 12h;
DOI:10.1248/cpb.55.1385

Reference yield:

: 112057-64-4
(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropan-1-ol

: 958882-67-2
(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropyl p-toluenesulfonyloxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 2 h / 20 °C

1.2: 72 percent / hydroxylamine hydrochloride; pyridine / 4 h / 20 °C

2.1: 43 percent / Et₃N / diethyl ether / 12 h / 20 °C

With triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1248/cpb.55.1385