(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

Base Information

Chemical Name:(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate
CAS No.:1309151-10-7
Molecular Formula:C₂₃H₃₃NS₂
Molecular Weight:387.654
Hs Code.:

Synonyms:(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

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Chemical Property of (2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

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Technology Process of (2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

There total 4 articles about (2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1-(4-(2,4,6-triisopropylphenyl)-1,3-dithiol-2-ylidene)piperidinium tetrafluoroborate

: 1309151-10-7
(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201100420

Reference yield:

: 110-89-4
piperidine

: 1309151-10-7
(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

Guidance literature:: Multi-step reaction with 4 steps

1: acetone / 0.5 h / 0 °C / Inert atmosphere

2: acetonitrile / 2 h / 80 °C / Inert atmosphere

3: tetrafluoroboric acid / water; acetic anhydride / 0.33 h / 20 °C / Inert atmosphere

4: potassium hexamethylsilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With tetrafluoroboric acid; potassium hexamethylsilazane; In tetrahydrofuran; water; acetic anhydride; acetone; acetonitrile;
DOI:10.1002/anie.201100420

Reference yield:

: 1309151-28-7
2-oxo-2-(2,4,6-triisopropylphenyl)ethyl piperidine-1-carbodithioate

: 1309151-10-7
(2,4,6-triisopropylphenyl)ethynyl piperidine-1-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrafluoroboric acid / water; acetic anhydride / 0.33 h / 20 °C / Inert atmosphere

2: potassium hexamethylsilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With tetrafluoroboric acid; potassium hexamethylsilazane; In tetrahydrofuran; water; acetic anhydride;
DOI:10.1002/anie.201100420