tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Base Information

• Chemical Name: tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate
• CAS No.: 1418150-19-2
• Molecular Formula: C₂₀H₂₅Cl₂N₅O₂S₂
• Molecular Weight: 502.489

Synonyms:tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Chemical Property of tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

There total 3 articles about tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.2%

tert-butyl-4-((prop-2-yn-1-ylthio)carbonothioyl)piperazine-1-carboxylate (1418150-39-6) + 4-(azidomethyl)-1,2-dichlorobenzene (99613-63-5) → tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-19-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1016/j.ejmech.2012.12.046

Reference yield:

1-t-Butoxycarbonylpiperazine (57260-71-6) → tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-19-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium phosphate dodecahydrate / acetone / 0.5 h / 20 °C

2: acetone / 0.5 h / 20 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

With sodium phosphate dodecahydrate; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.ejmech.2012.12.046

Reference yield:

C10H18N2O2S2 (773024-43-4) → tert butyl 4-(((1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 0.5 h / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.ejmech.2012.12.046

upstream raw materials:

tert-butyl-4-((prop-2-yn-1-ylthio)carbonothioyl)piperazine-1-carboxylate

4-(azidomethyl)-1,2-dichlorobenzene

C₁₀H₁₈N₂O₂S₂

1-t-Butoxycarbonylpiperazine

Downstream raw materials:

(1-(3,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methylpiperazine-1-carbodithioate

C₂₃H₂₃Cl₂N₅O₂S₂

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