5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

Base Information

Chemical Name:5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide
CAS No.:600730-95-8
Molecular Formula:C₂₁H₁₅F₄NO₄
Molecular Weight:421.348
Hs Code.:

Synonyms:5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

Chemical Property:

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Technology Process of 5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

There total 2 articles about 5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65399-05-5
5-amino-3H-isobenzofuran-1-one

: 3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionic acid chloride

: 600730-95-8
5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

Guidance literature:: In ISOPROPYLAMIDE; at 20 ℃; for 16h;

Reference yield:

: 65399-05-5
5-amino-3H-isobenzofuran-1-one

: 600730-94-7
3-[1-(2-Fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionic acid

: 600730-95-8
5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

Guidance literature:: With hydrogenchloride; thionyl chloride; In ISOPROPYLAMIDE; ethyl acetate;

Reference yield:

: 600730-95-8
5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 600730-96-9,600730-97-0,600730-98-1
()-5-{2-hydroxy-3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-trifluoromethyl-propionylamino}-phthalide

Guidance literature:: 5-{3-[1-(2-fluoro-5-trifluoromethylphenyl)-cyclopropyl]-2-oxo-propionylamino}-phthalide; (trifluoromethyl)trimethylsilane; With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 18h;

tetrabutyl ammonium fluoride; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 0 ℃; for 1h;