tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate)

Base Information

• Chemical Name: tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate)
• CAS No.: 856132-23-5
• Molecular Formula: C₈₂H₁₀₈N₆O₁₅
• Molecular Weight: 1417.79

Synonyms:tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate)

Chemical Property of tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate)

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Technology Process of tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate)

There total 1 articles about tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetra(tert-butyl) 2,2',2,2'-{[6-N-(4-methoxytrityl)hexylimino]bis(methylene)bis-(4-bromopyridine-6,2-diyl)bis(methylenenitrilo)}tetrakis(acetate) (856134-28-6) + (2,4,6-trimethoxyphenyl)boronic acid (135159-25-0) → tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate) (856132-23-5)

Guidance literature:

With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In DMF (N,N-dimethyl-formamide); at 95 ℃;

Reference yield: 100.0%

tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate) (856132-23-5) → C46H60N6O14 (856132-54-2)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 1h;

Reference yield: 74.0%

tetra(tertbutyl) 2,2',2,2'''-{[6-N-(4-methoxytrityl)aminohexyl-imino]bis(methylene)bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis(acetate) (856132-23-5) → tetra (tert-butyl) 2,2',2,2'''-{(6-aminohexylimino)bis(methylene)-bis[4-(2,4,6-trimethoxyphenyl)pyridine-6,2-diyl]bis(methylenenitrilo)}tetrakis-(acetate)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

upstream raw materials:

tetra(tert-butyl) 2,2',2,2'-{[6-N-(4-methoxytrityl)hexylimino]bis(methylene)bis-(4-bromopyridine-6,2-diyl)bis(methylenenitrilo)}tetrakis(acetate)

(2,4,6-trimethoxyphenyl)boronic acid

Downstream raw materials:

C₄₆H₆₀N₆O₁₄

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