Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester

Base Information

• Chemical Name: Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester
• CAS No.: 226921-20-6
• Molecular Formula: C₁₂H₂₁O₄PSe
• Molecular Weight: 339.23
• Mol file: 226921-20-6.mol

Synonyms:Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester

Chemical Property of Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester

There total 3 articles about Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-cyclohexenyl methyl ketone (932-66-1) → Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester (226921-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NEt₃, NaI

2: CH₂Cl₂ / 1 h / Ambient temperature

With triethylamine; sodium iodide; In dichloromethane;

DOI:10.1016/S0040-4039(99)00528-6

Reference yield:

1-cyclohexenyl methyl ketone (932-66-1) → Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester (226921-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NaI, Et₃N / acetonitrile

With triethylamine; sodium iodide; In acetonitrile;

DOI:10.1080/10426509608046285

Reference yield:

((1-(cyclohex-1-en-1-yl)vinyl)oxy)trimethylsilane (54781-35-0) + chloroselenotriethoxyphosphonium chlorosulfide → Selenophosphoric acid Se-(2-cyclohex-1-enyl-2-oxo-ethyl) ester O,O'-diethyl ester (226921-20-6)

Guidance literature:

DOI:10.1080/10426509608046285

upstream raw materials:

((1-(cyclohex-1-en-1-yl)vinyl)oxy)trimethylsilane

1-cyclohexenyl methyl ketone

Downstream raw materials:

1-vinylcyclohexene