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dihydroxy(2,4,6-triethylphenyl)borane

Base Information
  • Chemical Name:dihydroxy(2,4,6-triethylphenyl)borane
  • CAS No.:108593-75-5
  • Molecular Formula:C12H19BO2
  • Molecular Weight:206.093
  • Hs Code.:
dihydroxy(2,4,6-triethylphenyl)borane

Synonyms:dihydroxy(2,4,6-triethylphenyl)borane

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of dihydroxy(2,4,6-triethylphenyl)borane
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Technology Process of dihydroxy(2,4,6-triethylphenyl)borane

There total 1 articles about dihydroxy(2,4,6-triethylphenyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With magnesium; In tetrahydrofuran; diethyl ether; react. of organic compound with Mg in THF, addn. of obtained soln. to asoln. of B-compound in Et2O, stirring for 1 h (under inert gas); addn. of water, sepg. organic phase, washing (water, NaCl-soln.), drying (Na2SO4), removing solvent (vac.), recrystn. (n-hexane), elem. anal.;
Guidance literature:
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium hydroxide octahydrate; In water; toluene; at 110 ℃; for 15h; Inert atmosphere;
Guidance literature:
heating for 15 h at 100°C/5E-3 Torr (under inert gas); slow crystn., elem. anal.;
upstream raw materials:

Trimethyl borate

2-bromo-1,3,5-triethylbenzene

Downstream raw materials:

tris(2,4,6-triethylphenyl)boroxin

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