4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide

Base Information

• Chemical Name: 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide
• CAS No.: 1316304-09-2
• Molecular Formula: C₉H₁₁NS₃
• Molecular Weight: 229.391
• Mol file: 1316304-09-2.mol

Synonyms:4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide

Chemical Property of 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide

There total 2 articles about 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5-methyl-[1,3,5]dithiazinane (6302-94-9) + 4-aminotiophenol (1193-02-8) → 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide (1316304-09-2)

Guidance literature:

With samarium(III) nitrate hexahydrate; In ethanol; chloroform; at 60 ℃; for 3h; chemoselective reaction; Inert atmosphere;

DOI:10.1134/S1070428011090065

Reference yield: 65.0%

[1,3,5]trithiane (291-21-4) + 4-aminotiophenol (1193-02-8) → 4-(1,3,5-dithiazinan-5-yl)phenyl hydrosulfide (1316304-09-2)

Guidance literature:

With iron(III) chloride hexahydrate; In acetonitrile; at 60 ℃; for 6h; chemoselective reaction; Inert atmosphere;

DOI:10.1134/S1070428011090065

upstream raw materials:

[1,3,5]trithiane

4-aminotiophenol

5-methyl-[1,3,5]dithiazinane