22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine

Base Information

• Chemical Name: 22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine
• CAS No.: 675832-95-8
• Molecular Formula: C₃₂H₂₄N₈O₂S₂
• Molecular Weight: 616.727
• Mol file: 675832-95-8.mol

Synonyms:22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine

Chemical Property of 22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine

There total 1 articles about 22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

phthalonitrile (91-15-6) + (Z)-1,2-bis(2-hydroxyethylthio)ethene-1,2-dicarbonitrile → 29H,31H-Phthalocyanine (574-93-6) + 22,23-di(2-hydroxyethylthio)-μ-27H,29H-tribenzo[b,g,l]porphyrazine (675832-95-8)

Guidance literature:

phthalonitrile; (Z)-1,2-bis(2-hydroxyethylthio)ethene-1,2-dicarbonitrile; With iodine; magnesium; In butan-1-ol; for 12h; Heating;

With trifluoroacetic acid; at 20 ℃; for 3h;

DOI:10.1007/s00706-003-0074-5

upstream raw materials:

phthalonitrile