Technology Process of 6-methyl-3-phenylhydrocoumarin
There total 3 articles about 6-methyl-3-phenylhydrocoumarin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% Pd/C; hydrogen;
In
ethyl acetate;
at 20 ℃;
under 750.075 Torr;
DOI:10.1021/ja3096202
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride / benzene / 24 h / 20 °C
2: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 20 °C
3: hydrogen; 10% Pd/C / ethyl acetate / 20 °C / 750.08 Torr
With
oxalyl dichloride; 10% Pd/C; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate;
In
dichloromethane; water; ethyl acetate; benzene;
DOI:10.1021/ja3096202
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 20 °C
2: hydrogen; 10% Pd/C / ethyl acetate / 20 °C / 750.08 Torr
With
10% Pd/C; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate;
In
dichloromethane; water; ethyl acetate;
DOI:10.1021/ja3096202
