2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

Base Information

Chemical Name:2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine
CAS No.:77092-62-7
Molecular Formula:C₂₆H₃₃NO₅
Molecular Weight:439.552
Hs Code.:

Synonyms:2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

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Chemical Property of 2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

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Technology Process of 2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

There total 3 articles about 2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 77092-59-2
2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-MEMoxy-4'-methoxyphenyl)(e)-trans-quinolizidine

: 77092-62-7
2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/0040-4020(80)85040-X

Reference yield:

: 69730-94-5,69730-95-6,82929-78-0,82929-79-1
(2S,9aS)-4-[4-Methoxy-3-(2-methoxy-ethoxymethoxy)-phenyl]-octahydro-quinolizin-2-ol

: 77092-62-7
2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium hydride / xylene / 6 h / Heating

2: 80 percent / trifluoroacetic acid (TFA) / CH₂Cl₂ / 2 h / 0 °C

With sodium hydride; trifluoroacetic acid; In dichloromethane; xylene;
DOI:10.1016/0040-4020(80)85040-X

Reference yield:

: 15823-04-8
methyl 3-(4-methoxyphenyl)propionate

: 77092-62-7
2-(p-methoxyphenylpropionoyloxy)(a)-4-(3'-hydroxy-4'-methoxyphenyl)(e)-trans-quinolizidine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium hydride / xylene / 6 h / Heating

2: 80 percent / trifluoroacetic acid (TFA) / CH₂Cl₂ / 2 h / 0 °C

With sodium hydride; trifluoroacetic acid; In dichloromethane; xylene;
DOI:10.1016/0040-4020(80)85040-X