2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

Base Information

Chemical Name:2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine
CAS No.:222192-36-1
Molecular Formula:C₃₆H₅₀Br₂N₂O₁₂
Molecular Weight:862.607
Hs Code.:

Synonyms:2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

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Chemical Property of 2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

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Technology Process of 2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

There total 1 articles about 2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 222192-35-0
(2-{2-[3-(3-hydroxypropoxy)-2-di-(ethoxycarbonylmethyl)aminophenoxy]ethoxy}-6-(3-hydroxypropoxy)-N,N-di(ethoxycarbonylmethyl)benzenamine)

: 222192-36-1
2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In diethyl ether;
DOI:10.1021/ja983702l

Reference yield: 80.0%

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 222192-36-1
2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

: 222192-37-2
({2-(2-{2-(Bis-ethoxycarbonylmethyl-amino)-3-[3-(1,4,7,10-tetraaza-cyclododec-1-yl)-propoxy]-phenoxy}-ethoxy)-6-[3-(1,4,7,10-tetraaza-cyclododec-1-yl)-propoxy]-phenyl}-ethoxycarbonylmethyl-amino)-acetic acid ethyl ester

Guidance literature:: In chloroform;
DOI:10.1021/ja983702l

Reference yield:

: 222192-36-1
2-{2-[3-(3-bromopropoxy)-2-di(ethoxycarbonylmethyl)-aminophenoxy]ethoxy}-6-(3-bromopropoxy)-N,N-di-(ethoxycarbonylmethyl)benzenamine

: ({2-(2-{2-(Bis-carboxymethyl-amino)-3-[3-(4,7,10-tris-carboxymethyl-1,4,7,10-tetraaza-cyclododec-1-yl)-propoxy]-phenoxy}-ethoxy)-6-[3-(4,7,10-tris-carboxymethyl-1,4,7,10-tetraaza-cyclododec-1-yl)-propoxy]-phenyl}-carboxymethyl-amino)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / CHCl₃

2: 82 percent / NaOH

With sodium hydroxide; In chloroform;
DOI:10.1021/ja983702l