Technology Process of C17H14Cl2N2O3
There total 5 articles about C17H14Cl2N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl acetamide;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.09.046
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 4 h / 20 °C
2: triethylamine / 1,2-dichloro-ethane / 3 h / 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide / butanone / 4 h / Reflux
4: sodium hydride / N,N-dimethyl acetamide / 24 h / 20 °C / Inert atmosphere
With
palladium on activated charcoal; hydrogen; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; potassium iodide;
In
tetrahydrofuran; N,N-dimethyl acetamide; 1,2-dichloro-ethane; butanone;
DOI:10.1016/j.bmcl.2011.09.046
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / 1,2-dichloro-ethane / 3 h / 20 °C
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide / butanone / 4 h / Reflux
3: sodium hydride / N,N-dimethyl acetamide / 24 h / 20 °C / Inert atmosphere
With
sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; potassium iodide;
In
N,N-dimethyl acetamide; 1,2-dichloro-ethane; butanone;
DOI:10.1016/j.bmcl.2011.09.046
