2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

Base Information

Chemical Name:2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol
CAS No.:330183-96-5
Molecular Formula:C₁₁H₁₃NOSe
Molecular Weight:254.19
Hs Code.:

Synonyms:2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

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Chemical Property of 2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

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Technology Process of 2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

There total 3 articles about 2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 205828-75-7
bis[2-(4,4-dimethyl-2-oxazolinyl)phenyl] diselenide

: 330183-96-5
2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

Guidance literature:: bis[2-(4,4-dimethyl-2-oxazolinyl)phenyl] diselenide; With sodium tetrahydroborate; for 1h;

With hydrogenchloride; In methanol; Further stages.;
DOI:10.1021/ja994467p

Reference yield:

: 19312-06-2
4,5-dihydro-4,4-dimethyl-2-phenoxazole

: 330183-96-5
2-[4,4-dimethyl-2-oxazolinyl]phenyl selenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane / 1 h / 20 °C

1.2: Se / hexane / 2 h / 0 °C

1.3: 60 percent / O₂; aq. NaHCO₃ / hexane / 0.25 h

2.1: NaBH₄ / 1 h

2.2: aq. HCl / methanol

With sodium tetrahydroborate; n-butyllithium; In hexane;
DOI:10.1021/ja994467p