4-oxo-6-phenylhexanoic acid methyl ester

Base Information

Chemical Name:4-oxo-6-phenylhexanoic acid methyl ester
CAS No.:22187-89-9
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:4-oxo-6-phenylhexanoic acid methyl ester

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Chemical Property of 4-oxo-6-phenylhexanoic acid methyl ester

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Technology Process of 4-oxo-6-phenylhexanoic acid methyl ester

There total 8 articles about 4-oxo-6-phenylhexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103681-39-6
Se-methyl selenohydrocinnamate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 22187-89-9
4-oxo-6-phenylhexanoic acid methyl ester

: 19464-44-9
methyl 3-(tri-n-butylstannyl)propionate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.75h; Heating;
DOI:10.1021/ja00181a033

Reference yield: 91.0%

: 104869-92-3
5-Benzenesulfonyl-4-oxo-6-phenyl-hexanoic acid methyl ester

: 22187-89-9
4-oxo-6-phenylhexanoic acid methyl ester

Guidance literature:: With tris(2,2'-bipyridine)ruthenium dichloride; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In pyridine; for 20h; Ambient temperature; Irradiation;
DOI:10.1246/cl.1986.87

Reference yield: 80.0%

: 37904-38-4
5-phenylpent-1-en-3-ol

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 22187-89-9
4-oxo-6-phenylhexanoic acid methyl ester

Guidance literature:: 5-phenylpent-1-en-3-ol; acrylic acid methyl ester; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 110 ℃; for 0.5h; Inert atmosphere;

With sodium hydroxide; In toluene; at 130 ℃; for 3h; Reagent/catalyst;
DOI:10.1039/c3ob40167g