4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)
CAS No.:1393809-20-5
Molecular Formula:C₂₃H₂₂O₈S₂
Molecular Weight:490.555
Hs Code.:

Synonyms:4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

Suppliers and Price of 4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

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Technology Process of 4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

There total 2 articles about 4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 68097-14-3
4-acetyl-5-hydroxy-1,3-phenylene bis(4-methylbenzenesulfonate)

: 74-88-4
methyl iodide

: 1393809-20-5
4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

Guidance literature:: With potassium carbonate; In acetone; Inert atmosphere; Reflux;
DOI:10.5012/bkcs.2012.33.6.2087

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 98-59-9
p-toluenesulfonyl chloride

: 1393809-20-5
4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / Inert atmosphere; Reflux

2: potassium carbonate / acetone / Inert atmosphere; Reflux

With potassium carbonate; In acetone;
DOI:10.5012/bkcs.2012.33.6.2087

Reference yield: 92.0%

: 1393809-20-5
4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate)

: 3602-54-8
4,6-dihydroxy-2-methoxyacetophenone

Guidance literature:: 4-acetyl-5-methoxy-1,3-phenylene bis(4-methylbenzenesulfonate); With potassium carbonate; In methanol; Reflux; Inert atmosphere;

With hydrogenchloride; water; In methanol;
DOI:10.5012/bkcs.2012.33.6.2087