Cy₂PCH₂NHPh

Base Information

• Chemical Name: Cy₂PCH₂NHPh
• CAS No.: 1234313-16-6
• Molecular Formula: C₁₉H₃₀NP
• Molecular Weight: 303.428
• Mol file: 1234313-16-6.mol

Synonyms:Cy₂PCH₂NHPh

Chemical Property of Cy₂PCH₂NHPh

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cy₂PCH₂NHPh

There total 1 articles about Cy₂PCH₂NHPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

aniline (62-53-3) + hydroxymethyldicyclohexylphosphine (92031-76-0) → Cy2PCH2NHPh (1234313-16-6)

Guidance literature:

at -78 - 20 ℃; Inert atmosphere; Neat (no solvent);

DOI:10.1016/j.jorganchem.2010.03.006

Reference yield: 96.0%

Cy2PCH2NHPh (1234313-16-6) → Cy2PCH2NLiPh

Guidance literature:

With methyllithium; In toluene; at -78 ℃; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.03.006

Reference yield: 88.0%

Cy2PCH2NHPh (1234313-16-6) → Cy2P(S)CH2NHPh (1234313-19-9)

Guidance literature:

With sulfur; In toluene; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.03.006

upstream raw materials:

aniline

hydroxymethyldicyclohexylphosphine

Downstream raw materials:

Cy₂P(S)CH₂NHPh