C₂₀H₁₇NO₄

Base Information

Chemical Name:C₂₀H₁₇NO₄
CAS No.:1380109-75-0
Molecular Formula:C₂₀H₁₇NO₄
Molecular Weight:335.359
Hs Code.:

C<sub>20</sub>H<sub>17</sub>NO<sub>4</sub>

Synonyms:C₂₀H₁₇NO₄

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Chemical Property of C₂₀H₁₇NO₄

Chemical Property:

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Technology Process of C₂₀H₁₇NO₄

There total 5 articles about C₂₀H₁₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1380109-74-9
C₂₀H₁₉NO₄

: 1380109-75-0
C₂₀H₁₇NO₄

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 ℃; for 3h;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380109-75-0
C₂₀H₁₇NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / methanol; water / 0.17 h / Reflux

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

4: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C

With hydroxylamine hydrochloride; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; triethylamine; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jm400560z

Reference yield:

: 1380109-77-2
5-(benzyloxy)-1-hydroxy-2-(hydroxymethyl)pyridin-4(1H)-one

: 1380109-75-0
C₂₀H₁₇NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

2: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C

With sulfur trioxide pyridine complex; potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm400560z