3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

Base Information

Chemical Name:3-trimethylstannyl-N-diphenylmethylenealanine methyl ester
CAS No.:224964-12-9
Molecular Formula:C₂₀H₂₅NO₂Sn
Molecular Weight:430.134
Hs Code.:

Synonyms:3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

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Chemical Property of 3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

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Technology Process of 3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

There total 1 articles about 3-trimethylstannyl-N-diphenylmethylenealanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 23696-40-4
trimethylstannylmethyl iodide

: 224964-12-9
3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

Guidance literature:: With NaH; In tetrahydrofuran; byproducts: H2, NaI; (exclusion of air and moisture); addn. of the glycinate in THF at 0°C to NaH in THF, stirring (0°C, 30 min), addn. of the iodide in THF, warming to room temp., then reflux to the neutral reaction of themixture; filtration, solvent removal by distn., addn. of benzene, filtration, removal of benzene, addn. of Et2O/petroleum ether, filtration, removal of solvents, distn. in vacuo;

Reference yield: 80.0%

: 224964-12-9
3-trimethylstannyl-N-diphenylmethylenealanine methyl ester

: 753-73-1
dimethyltin dichloride

: 3-chlor(dimethyl)stannyl-N-diphenylmethylenealanine methyl ester

Guidance literature:: In neat (no solvent); byproducts: Me3SnCl; (exclusion of air and moisture); 60°C, ca. 50 h; removal of volatiles (vac.), addn. of petroleum ether, filtration, evapn.;