sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

Base Information

Chemical Name:sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine
CAS No.:128524-87-8
Molecular Formula:C₁₂H₁₄NO₆S*Na
Molecular Weight:323.302
Hs Code.:

Synonyms:sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

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Chemical Property of sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

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Technology Process of sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

There total 5 articles about sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114791-24-1
diethyl 2-(acetylamino)-2-<<4-(chloromethyl)phenyl>methyl>propanedioic acid

: 128524-87-8
sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

Guidance literature:: With hydrogenchloride; sodium hydroxide; sodium sulfite; Yield given. Multistep reaction; 1.) 120 deg C, 3 h, 2.) 120 deg C, 1 h;
DOI:10.1021/jo00250a043

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 128524-87-8
sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / H₂, concd. aq. HCl / 10percent Pd/C / ethanol / 22 h / 760 Torr / Ambient temperature

2: 89 percent / NaNO₂, water / 2 h / 110 °C

3: 72 percent / thionyl chloride / CH₂Cl₂ / 23 h / Heating

4: 1.) sodium sulfite, 10percent aq. sodium hydroxide, 2.) 1 M aq. HCl / 1.) 120 deg C, 3 h, 2.) 120 deg C, 1 h

With hydrogenchloride; sodium hydroxide; thionyl chloride; water; hydrogen; sodium sulfite; sodium nitrite; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo00250a043

Reference yield:

: 17201-43-3
4-cyanobenzyl bromide

: 128524-87-8
sodium N-acetamido-p-(sulfomethyl)-DL-phenylalanine

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / Na / ethanol / 17 h / 110 °C

2: 85 percent / H₂, concd. aq. HCl / 10percent Pd/C / ethanol / 22 h / 760 Torr / Ambient temperature

3: 89 percent / NaNO₂, water / 2 h / 110 °C

4: 72 percent / thionyl chloride / CH₂Cl₂ / 23 h / Heating

5: 1.) sodium sulfite, 10percent aq. sodium hydroxide, 2.) 1 M aq. HCl / 1.) 120 deg C, 3 h, 2.) 120 deg C, 1 h

With hydrogenchloride; sodium hydroxide; thionyl chloride; water; hydrogen; sodium; sodium sulfite; sodium nitrite; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo00250a043