selaginpulvilin A

Base Information

Chemical Name:selaginpulvilin A
CAS No.:1510810-60-2
Molecular Formula:C₃₄H₂₄O₅
Molecular Weight:512.562
Hs Code.:

Synonyms:selaginpulvilin A

Suppliers and Price of selaginpulvilin A

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Chemical Property of selaginpulvilin A

Chemical Property:

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Technology Process of selaginpulvilin A

There total 9 articles about selaginpulvilin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: C₄₂H₃₂O₈

: 1510810-60-2
selaginpulvilin A

: 1510810-61-3
C₃₄H₂₂O₅

Guidance literature:: C₄₂H₃₂O₈; With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 80 ℃; for 12h; Inert atmosphere;

With potassium hydroxide; In 1,4-dioxane; water; at 40 ℃; for 1h;

Reference yield:

: C₁₆H₁₅BrO₃

: 1510810-60-2
selaginpulvilin A

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanesulfonic acid / water / 65 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 120 °C / Inert atmosphere

3.1: tetrahydrofuran / Inert atmosphere; Cooling with ice

4.1: methanesulfonic acid / dichloromethane / 20 °C

5.1: boron tribromide / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere

6.1: pyridine / 12 h / 20 °C

7.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 12 h / 80 °C / Inert atmosphere

7.2: 1 h / 40 °C

With pyridine; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonic acid; 2,2'-azobis(isobutyronitrile); boron tribromide; triethylamine; triphenylphosphine; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 7-methoxy-9-(4-methoxyphenyl)-1-((4-methoxyphenyl)ethynyl)-2-methyl-9H-fluoren-9-ol

: 1510810-60-2
selaginpulvilin A

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonic acid / dichloromethane / 20 °C

2.1: boron tribromide / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere

3.1: pyridine / 12 h / 20 °C

4.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 12 h / 80 °C / Inert atmosphere

4.2: 1 h / 40 °C

With pyridine; N-Bromosuccinimide; methanesulfonic acid; 2,2'-azobis(isobutyronitrile); boron tribromide; In tetrachloromethane; dichloromethane;