selaginpulvilin C

Base Information

• Chemical Name: selaginpulvilin C
• CAS No.: 1510810-62-4
• Molecular Formula: C₃₄H₂₄O₄
• Molecular Weight: 496.562
• Mol file: 1510810-62-4.mol

Synonyms:selaginpulvilin C

Chemical Property of selaginpulvilin C

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of selaginpulvilin C

There total 9 articles about selaginpulvilin C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

4-(7-methoxy-9-(4-methoxyphenyl)-1-((4-methoxyphenyl)ethynyl)-2-methyl-9H-fluoren-9-yl)phenol → selaginpulvilin C (1510810-62-4)

Guidance literature:

With methyl magnesium iodide; In diethyl ether; at 160 ℃; for 1.08333h;

DOI:10.1021/acs.orglett.6b03241

Reference yield:

C27H26O3Si → selaginpulvilin C (1510810-62-4)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrahydrofuran / 0.25 h / 5 - 25 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 5 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 5 °C

4: methyl magnesium iodide / diethyl ether / 1.08 h / 160 °C

With methyl magnesium iodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1021/acs.orglett.6b03241

Reference yield:

C34H34O4Si → selaginpulvilin C (1510810-62-4)

Guidance literature:

Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 5 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 5 °C

3: methyl magnesium iodide / diethyl ether / 1.08 h / 160 °C

With methyl magnesium iodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1021/acs.orglett.6b03241

upstream raw materials:

4-methoxyphenyl magnesium bromide

3-methyl-2-bromobenzoic acid

Downstream raw materials:

selaginpulvilin A

C₃₄H₂₂O₅

4,4'-(7-hydroxy-1-((4-hydroxyphenyl)ethynyl)-9H-fluorene-9,9-diyl)diphenol