selaginpulvilin C

Base Information

Chemical Name:selaginpulvilin C
CAS No.:1510810-62-4
Molecular Formula:C₃₄H₂₄O₄
Molecular Weight:496.562
Hs Code.:

Synonyms:selaginpulvilin C

Suppliers and Price of selaginpulvilin C

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of selaginpulvilin C

Chemical Property:

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Technology Process of selaginpulvilin C

There total 9 articles about selaginpulvilin C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 4-(7-methoxy-9-(4-methoxyphenyl)-1-((4-methoxyphenyl)ethynyl)-2-methyl-9H-fluoren-9-yl)phenol

: 1510810-62-4
selaginpulvilin C

Guidance literature:: With methyl magnesium iodide; In diethyl ether; at 160 ℃; for 1.08333h;
DOI:10.1021/acs.orglett.6b03241

Reference yield:

: C₂₇H₂₆O₃Si

: 1510810-62-4
selaginpulvilin C

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 0.25 h / 5 - 25 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 5 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 5 °C

4: methyl magnesium iodide / diethyl ether / 1.08 h / 160 °C

With methyl magnesium iodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/acs.orglett.6b03241

Reference yield:

: C₃₄H₃₄O₄Si

: 1510810-62-4
selaginpulvilin C

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 5 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 5 °C

3: methyl magnesium iodide / diethyl ether / 1.08 h / 160 °C

With methyl magnesium iodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/acs.orglett.6b03241