N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide

Base Information

• Chemical Name: N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide
• CAS No.: 1024003-97-1
• Molecular Formula: C₂₁H₂₃F₂N₃O₂
• Molecular Weight: 387.429

Synonyms:N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide

Chemical Property of N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide

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Technology Process of N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide

There total 1 articles about N₅-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C15H11ClF2N2O (1024006-07-2) + 1-amino-3,3-dimethylbutan-2-one hydrochloride (33119-72-1) → N5-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carboxamide (1024003-97-1)

Guidance literature:

With triethylamine; dmap; In dichloromethane; at 0 - 35 ℃; for 8.25 - 16.25h;

Reference yield: 89.0%

N5-(3,3-dimethyl-2-oxobutyl)-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carboxamide (1024003-97-1) → 5-(tert-butyl)-2-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3yl]-1,3-oxazole (1024004-14-5)

Guidance literature:

With trichlorophosphate; for 8 - 16h; Heating / reflux;

upstream raw materials:

C₁₅H₁₁ClF₂N₂O

1-amino-3,3-dimethylbutan-2-one hydrochloride

Downstream raw materials:

5-(tert-butyl)-2-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3yl]-1,3-oxazole

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