N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone
CAS No.:1033192-77-6
Molecular Formula:C₁₉H₂₃NO₄S
Molecular Weight:361.462
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Suppliers and Price of N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

There total 3 articles about N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1-(1-benzenesulfinyl-ethyl)-4,4-dimethoxy-cyclohexa-2,5-dienyl]-carbamic acid tert-butyl ester

: 1033192-77-6
N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Guidance literature:: With oxalic acid; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/b414666b

Reference yield:

: 18437-68-8
tert-butyl N-(4-methoxyphenyl)carbamate

: 1033192-77-6
N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / LiClO₄; pyridine / 0 °C / anodic oxidation

2: LDA / tetrahydrofuran / -78 - 20 °C

3: aq. oxalic acid / tetrahydrofuran / 20 °C

With pyridine; lithium perchlorate; oxalic acid; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1039/b414666b

Reference yield:

: 106501-78-4
tert-butyl (4,4-dimethoxycyclohexa-2,5-dien-1-ylidene)carbamate

: 1033192-77-6
N-(tert-butoxycarbonyl)-4-amino-4-[(1'-methyl-1'-benzenesulfonyl)methyl]-2,5-cyclohexadienone

Guidance literature:: Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran / -78 - 20 °C

2: aq. oxalic acid / tetrahydrofuran / 20 °C

With oxalic acid; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1039/b414666b