methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Base Information

Chemical Name:methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate
CAS No.:325469-98-5
Molecular Formula:C₂₇H₃₆N₂O₁₂S
Molecular Weight:612.655
Hs Code.:

Synonyms:methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

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Chemical Property of methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

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Technology Process of methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

There total 3 articles about methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 178685-40-0
methyl (S-4-nitrobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

: 325469-98-5
methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Guidance literature:: With tin(ll) chloride; In ethanol; at 70 ℃; for 15h;
DOI:10.1016/S0968-0896(00)00201-7

Reference yield:

: 104556-69-6
2-Thiosialic acid methyl ester peracetate

: 325469-98-5
methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazinium acetate / dimethylformamide / 0.5 h / 20 °C

1.2: 67 percent / Et₃N / dimethylformamide / 2 h / 20 °C

2.1: 55 percent / SnCl₂*2H₂O / ethanol / 15 h / 70 °C

With hydrazinium monoacetate; tin(ll) chloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(00)00201-7

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 325469-98-5
methyl (S-4-aminobenzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazinium acetate / dimethylformamide / 0.5 h / 20 °C

1.2: 67 percent / Et₃N / dimethylformamide / 2 h / 20 °C

2.1: 55 percent / SnCl₂*2H₂O / ethanol / 15 h / 70 °C

With hydrazinium monoacetate; tin(ll) chloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(00)00201-7