4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine

Base Information

• Chemical Name: 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine
• CAS No.: 474917-94-7
• Molecular Formula: C₂₃H₂₆N₂O₇
• Molecular Weight: 442.469

Synonyms:4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine

Chemical Property of 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine

Chemical Property:

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Technology Process of 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine

There total 1 articles about 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

morpholine (110-91-8,99108-56-2) + allyl 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalaninate (474917-93-6) → 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine (474917-94-7)

Guidance literature:

Pd(Ph₃P)4; In dichloromethane;

Reference yield:

4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine (474917-94-7) + O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate (125700-67-6) + methyl 2-(4-aminobutoxy)-6-hydroxybenzoate (436864-53-8) → methyl 2-(4-{[4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanyl]amino}butoxy)-6-hydroxybenzoate (474917-96-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

4-{[(benzyloxy)(oxo)acetyl]amino}-N-(methoxycarbonyl)-L-phenylalanine (474918-00-8) + 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanine (474917-94-7) → 2-(4-{[4-[(carboxycarbonyl)amino]-N-(methoxycarbonyl)-L-phenylalanyl]amino}butoxy)-6-hydroxybenzoic acid

Guidance literature:

upstream raw materials:

morpholine

allyl 4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalaninate

Downstream raw materials:

methyl 2-(4-{[4-{[(benzyloxy)(oxo)acetyl]amino}-N-(tert-butoxycarbonyl)-L-phenylalanyl]amino}butoxy)-6-hydroxybenzoate

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