5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

Base Information

Chemical Name:5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide
CAS No.:1253733-72-0
Molecular Formula:C₁₈H₁₃F₂IN₄O₂S
Molecular Weight:514.294
Hs Code.:

Synonyms:5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

Suppliers and Price of 5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

There total 6 articles about 5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1253733-71-9
5-(2,6-difluorophenyl)-7-iodo-1H-pyrazolo[4,3-c]isoquinoline

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1253733-72-0
5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

: 1253733-73-1
5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-2-sulphonic acid dimethylamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 1253733-68-4
3-(4-iodophenyl)-1H-pyrazol-4-ylamine

: 1253733-72-0
5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 20 °C

2.1: phosphorus pentoxide / 23 h / 165 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C

With phosphorus pentoxide; sodium hydride; sodium hydroxide; In tetrahydrofuran; ethanol; water; mineral oil;

Reference yield:

: 1253733-68-4
3-(4-iodophenyl)-1H-pyrazol-4-ylamine

: 1253733-72-0
5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-1-sulphonic acid dimethylamide

: 1253733-73-1
5-(2,6-difluorophenyl)-7-iodopyrazolo[4,3-c]isoquinoline-2-sulphonic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 20 °C

2.1: phosphorus pentoxide / 23 h / 165 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1.5 h / 0 °C / Inert atmosphere

With phosphorus pentoxide; sodium hydride; sodium hydroxide; In tetrahydrofuran; ethanol; water; mineral oil;