(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

Base Information

Chemical Name:(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan
CAS No.:147588-02-1
Molecular Formula:C₁₇H₁₈O
Molecular Weight:238.329
Hs Code.:

(+/-)-6-oxo-5-(benzylidene-(ξ))-(3a<i>rH</i>.7a<i>cH</i>)-hexahydro-4<i>t</i>.7<i>t</i>-methano-indan

Synonyms:(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

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Chemical Property of (+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

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Technology Process of (+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

There total 5 articles about (+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 34748-64-6
exo-2,exo-6-tricyclo[5.2.1.0^2.6]decan-8-one

: 100-52-7
benzaldehyde

: 147588-02-1
(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

Guidance literature:: With potassium hydroxide; In ethanol; for 24h;
DOI:10.1016/S0014-827X(98)00008-1

Reference yield:

: 10271-42-8,10271-43-9,10271-44-0,10271-45-1,13380-89-7,131408-34-9,15904-95-7
Octahydro-endo-4,7-methanoinden-endo-5-ol

: 147588-02-1
(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃; acetic acid / 95 °C

2: aq.-ethanolic NaOH / 15 °C

With chromium(VI) oxide; sodium hydroxide; acetic acid;
DOI:10.1177/0739986302024003001

Reference yield:

: 2826-19-9
(3aR^*,4S^*,7R^*,7aS^*)-2,3,3a,4,7,7a-hexahydro-4,7-methano-1H-indene

: 147588-02-1
(+/-)-6-oxo-5-(benzylidene-(ξ))-(3arH.7acH)-hexahydro-4t.7t-methano-indan

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous H₂SO₄

2: CrO₃; acetic acid / 95 °C

3: aq.-ethanolic NaOH / 15 °C

With chromium(VI) oxide; sodium hydroxide; sulfuric acid; acetic acid;
DOI:10.1177/0739986302024003001