1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene

Base Information

Chemical Name:1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene
CAS No.:263389-18-0
Molecular Formula:C₁₉H₁₅NO₂S
Molecular Weight:321.4
Hs Code.:2926909090
DSSTox Substance ID:DTXSID80378057
Mol file:263389-18-0.mol

Synonyms:263389-18-0;1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene;1-(isocyano(tosyl)methyl)naphthalene;1-[isocyano-(4-methylphenyl)sulfonylmethyl]naphthalene;1-[isocyano(4-methylbenzenesulfonyl)methyl]naphthalene;MFCD06245435;Naphthalene, 1-[isocyano[(4-methylphenyl)sulfonyl]methyl]-;DTXSID80378057;AKOS005257520;GS-0342;A5231;FT-0604129;1-[Isocyano(toluene-4-sulphonyl)methyl]naphthalene;1-[isocyano-(toluene-4-sulfonyl)methyl]naphthalene;1-[Isocyano(4-methylbenzene-1-sulfonyl)methyl]naphthalene

Suppliers and Price of 1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-[ISOCYANO-(TOLUENE-4-SULFONYL)-METHYL]-NAPHTHALENE 95.00%
1G
$ 1086.86

American Custom Chemicals Corporation
1-[ISOCYANO-(TOLUENE-4-SULFONYL)-METHYL]-NAPHTHALENE 95.00%
500MG
$ 960.25

American Custom Chemicals Corporation
1-[ISOCYANO-(TOLUENE-4-SULFONYL)-METHYL]-NAPHTHALENE 95.00%
50MG
$ 752.14

Total 9 raw suppliers

Chemical Property of 1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：42.52000
Density:g/cm³
LogP:4.85150
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:321.08234989
Heavy Atom Count:23
Complexity:548

Purity/Quality:

97% ^*data from raw suppliers

1-[ISOCYANO-(TOLUENE-4-SULFONYL)-METHYL]-NAPHTHALENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:T

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C(C2=CC=CC3=CC=CC=C32)[N+]#[C-]

Technology Process of 1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene

There total 3 articles about 1-[Isocyano-(toluene-4-sulfonyl)-methyl]-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 671776-97-9
N-((2-naphthyl)(tosyl)methyl)formamide

: 263389-18-0
[(4-methylphenyl)sulfonyl]naphthylmethanisocyanide

Guidance literature:: With triethylamine; trichlorophosphate; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1039/c9ob00660e

Reference yield:

: 536-57-2
p-toluene sulfinic acid

: 263389-18-0
[(4-methylphenyl)sulfonyl]naphthylmethanisocyanide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile; toluene / 16 h / 55 °C

2: trichlorophosphate; triethylamine / tetrahydrofuran / 0.5 h / 0 °C

With triethylamine; trichlorophosphate; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1039/c9ob00660e

Reference yield:

: 824-79-3
sodium 4-methylbenzenesulfinate

: 263389-18-0
[(4-methylphenyl)sulfonyl]naphthylmethanisocyanide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; tert-butyl methyl ether / 20 °C

2: acetonitrile; toluene / 16 h / 55 °C

3: trichlorophosphate; triethylamine / tetrahydrofuran / 0.5 h / 0 °C

With hydrogenchloride; triethylamine; trichlorophosphate; In tetrahydrofuran; tert-butyl methyl ether; water; toluene; acetonitrile;
DOI:10.1039/c9ob00660e