2,6-dideuteriotoluene

Base Information

Chemical Name:2,6-dideuteriotoluene
CAS No.:80515-60-2
Molecular Formula:C₇H₈
Molecular Weight:94.1246
Hs Code.:

Synonyms:2,6-dideuteriotoluene

Suppliers and Price of 2,6-dideuteriotoluene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-dideuteriotoluene

Chemical Property:

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Technology Process of 2,6-dideuteriotoluene

There total 5 articles about 2,6-dideuteriotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 69321-60-4
2,6-dibromotoluene

: 80515-60-2
2,6-dideuteriotoluene

Guidance literature:: With lithium aluminium deuteride; In diethyl ether; at 80 ℃;
DOI:10.1002/jms.1089

Reference yield:

: 80515-68-0
2,6-dideuterio-4-aminotoluene

: 80515-60-2
2,6-dideuteriotoluene

Guidance literature:: With hypophosphoric acid; copper(l) chloride;
DOI:10.1016/S0040-4039(00)98745-8

Reference yield:

: 99-99-0
1-methyl-4-nitrobenzene

: 80515-60-2
2,6-dideuteriotoluene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / D₂SO₄ / 85 - 90 °C

2: 68 percent / tin, 38percent HCl / 0.5 h / 75 °C

3: 1.) conc. HCl, H₂O, NaNO₂, 2.) 50percent H₃PO₄ / 1.) 5-8 deg C, 0.5 h, 2.) 5 deg C, 24 h

With hydrogenchloride; tin; phosphoric acid; water; sulfuric acid-d2; sodium nitrite;
DOI:10.1021/jo00346a020