Technology Process of C29H35N9O3
There total 11 articles about C29H35N9O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 30 °C
2: 1-methyl-pyrrolidin-2-one / 4 h / 80 °C
3: hydrogenchloride / 60 °C
4: hydrogenchloride; water / ethanol / 20 °C
5: sodium hydroxide; water / tetrahydrofuran / 5 h / 20 °C
6: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C
With
hydrogenchloride; water; triethylamine; 3-chloro-benzenecarboperoxoic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / 60 °C
2: hydrogenchloride; water / ethanol / 20 °C
3: sodium hydroxide; water / tetrahydrofuran / 5 h / 20 °C
4: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C
With
hydrogenchloride; water; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;