(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

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Chemical Name:(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid
CAS No.:197972-09-1
Molecular Formula:C₃₄H₄₅F₃N₈O₁₇
Molecular Weight:894.77
Hs Code.:

(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

Synonyms:(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

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Chemical Property of (S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

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Technology Process of (S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

There total 3 articles about (S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2268-15-7
2,3,5-trifluorophenol

: 197972-09-1
(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: NH4OAc, tyrosine phenollylase, pyridoxal-5'-phosphate, β-mercaptoethanol, NH4OH / H2O / Ambient temperature

2: 10percent aq. Na₂CO₃ / dioxane / Ambient temperature

With ammonium hydroxide; tyrosine phenollylase; pyridoxal 5'-phosphate; ammonium acetate; sodium carbonate; 2-hydroxyethanethiol; In 1,4-dioxane; water;
DOI:10.1021/ja9808393

Reference yield:

: 182756-63-4
2,3,6-F₃Y

: 197972-09-1
(S)-4-{(S)-2-[(S)-2-((S)-2-Amino-4-carboxy-butyrylamino)-3-carboxy-propionylamino]-3-carbamoyl-propionylamino}-4-[(S)-1-[(1S,2R)-1-((S)-1-carboxy-ethylcarbamoyl)-2-hydroxy-propylcarbamoyl]-2-(2,3,6-trifluoro-4-hydroxy-phenyl)-ethylcarbamoyl]-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent aq. Na₂CO₃ / dioxane / Ambient temperature

With sodium carbonate; In 1,4-dioxane;
DOI:10.1021/ja9808393