C₆₀H₉₂O₉SSi₂

Base Information

Chemical Name:C₆₀H₉₂O₉SSi₂
CAS No.:1268269-25-5
Molecular Formula:C₆₀H₉₂O₉SSi₂
Molecular Weight:1045.62
Hs Code.:

C<sub>60</sub>H<sub>92</sub>O<sub>9</sub>SSi<sub>2</sub>

Synonyms:C₆₀H₉₂O₉SSi₂

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Chemical Property of C₆₀H₉₂O₉SSi₂

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Technology Process of C₆₀H₉₂O₉SSi₂

There total 19 articles about C₆₀H₉₂O₉SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 924656-50-8
C₇₀H₁₁₆O₁₀Si₄

: 75-08-1
ethanethiol

: 1268269-25-5
C₆₀H₉₂O₉SSi₂

Guidance literature:: With zinc trifluoromethanesulfonate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: C₇₀H₁₁₈O₁₀Si₄

: 1268269-25-5
C₆₀H₉₂O₉SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

2: zinc trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere

With tetrapropylammonium perruthennate; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; In dichloromethane;
DOI:10.1021/ja200089f

Reference yield:

: C₃₃H₄₆O₅Si

: 1268269-25-5
C₆₀H₉₂O₉SSi₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 6 h / 20 °C / Inert atmosphere

4.1: lead(IV) tetraacetate / benzene / 0.5 h / 20 °C / Inert atmosphere

5.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

6.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / Inert atmosphere

7.1: tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc / dichloromethane / 2 h / 65 °C / Inert atmosphere

7.2: 16 h / 80 °C

8.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

9.1: zinc trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere

With tetrahydrofuran; dmap; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; 2-methyl-6-nitrobenzoic anhydride; water; lead(IV) tetraacetate; titanium tetrachloride; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lead(II) chloride; zinc; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; benzene;
DOI:10.1021/ja200089f