4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

Base Information

Chemical Name:4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide
CAS No.:1443125-02-7
Molecular Formula:C₂₉H₃₄N₆O₄
Molecular Weight:530.627
Hs Code.:

Synonyms:4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

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Chemical Property of 4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

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Technology Process of 4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

There total 4 articles about 4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63214-57-3
(morpholin-4-yl)(piperidin-4-yl)methanone

: 32315-10-9
bis(trichloromethyl) carbonate

: C₁₈H₁₈N₄O

: 1443125-02-7
4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2013.01.056

Reference yield:

: 1403986-23-1
C₁₁H₁₁N₃O

: 1443125-02-7
4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 40 - 50 °C

2: acetic acid; iron / ethanol / 5 h / 120 °C

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With iron; caesium carbonate; acetic acid; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.01.056

Reference yield:

: C₁₈H₁₆N₄O₃

: 1443125-02-7
4-(morpholine-4-carbonyl)-N-(3-((6-oxo-3-(o-tolylamino)pyridazin-1(6H)-yl)methyl) phenyl)piperidine-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; iron / ethanol / 5 h / 120 °C

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With iron; acetic acid; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2013.01.056