6-Methyl-2-(methylthio)benzo[d]thiazole

Base Information

Chemical Name:6-Methyl-2-(methylthio)benzo[d]thiazole
CAS No.:3507-35-5
Molecular Formula:C9H9 N S2
Molecular Weight:195.309
Hs Code.:
DSSTox Substance ID:DTXSID201291260
Mol file:3507-35-5.mol

Synonyms:3507-35-5;6-Methyl-2-(methylthio)benzo[d]thiazole;SCHEMBL7867881;DTXSID201291260;6-Methyl-2-(methylthio)benzothiazole

Suppliers and Price of 6-Methyl-2-(methylthio)benzo[d]thiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 6-Methyl-2-(methylthio)benzo[d]thiazole

Chemical Property:

Boiling Point:319.8±35.0 °C(Predicted)
PKA:1.70±0.10(Predicted)
PSA：66.43000
Density:1.27±0.1 g/cm3(Predicted)
LogP:3.32660
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:195.01764164
Heavy Atom Count:12
Complexity:163

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)N=C(S2)SC

Technology Process of 6-Methyl-2-(methylthio)benzo[d]thiazole

There total 6 articles about 6-Methyl-2-(methylthio)benzo[d]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140-89-6
potassium ethyl xanthogenate

: 74-88-4
methyl iodide

: 3507-35-5
6-methyl-2-(methylthio)benzo[d]thiazole

Guidance literature:: potassium ethyl xanthogenate; 4-methyl-2-haloaniline; In N,N-dimethyl-formamide; at 140 ℃; for 4h;

methyl iodide; With triethylamine; In ethanol; at 80 ℃; for 1h;
DOI:10.1021/acs.jmedchem.8b00583

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 140-89-6
potassium ethyl xanthogenate

: 74-88-4
methyl iodide

: 3507-35-5
6-methyl-2-(methylthio)benzo[d]thiazole

Guidance literature:: 2-bromo-p-toluidine; potassium ethyl xanthogenate; In N,N-dimethyl-formamide; at 140 ℃; for 12h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1002/anie.201802369

Reference yield:

: 3507-26-4
2-chloro-6-methylbenzo[d]thiazole

: 3507-35-5
6-methyl-2-(methylthio)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; NaHS

2: methanol

With methanol; sodium hydrogensulfide; ethanol;
DOI:10.1039/jr9360001672