3-O-(imidazolylthiocarbonyl)-mesaconitine

Base Information

Chemical Name:3-O-(imidazolylthiocarbonyl)-mesaconitine
CAS No.:121236-31-5
Molecular Formula:C₃₇H₄₇N₃O₁₁S
Molecular Weight:741.86
Hs Code.:

Synonyms:3-O-(imidazolylthiocarbonyl)-mesaconitine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-(imidazolylthiocarbonyl)-mesaconitine

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-O-(imidazolylthiocarbonyl)-mesaconitine

There total 3 articles about 3-O-(imidazolylthiocarbonyl)-mesaconitine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2752-64-9
mesaconitine

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 121236-31-5
3-O-(imidazolylthiocarbonyl)-mesaconitine

Guidance literature:: In 1,2-dichloro-ethane; at 80 ℃; for 2.5h;
DOI:10.1016/S0040-4020(01)86133-0

Reference yield:

: 3327-35-3
N-desethylaconitine

: 121236-31-5
3-O-(imidazolylthiocarbonyl)-mesaconitine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / CaCO₃ / diethyl ether; methanol / 2 h / Heating

2: 97 percent / 1,2-dichloro-ethane / 2.5 h / 80 °C

With calcium carbonate; In methanol; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)86133-0

Reference yield:

: 302-27-2,140188-61-0
indaconitine

: 121236-31-5
3-O-(imidazolylthiocarbonyl)-mesaconitine

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / K₂CO₃, KMnO₄ / H₂O; acetone / 0.5 h / Ambient temperature

2: 90 percent / CaCO₃ / diethyl ether; methanol / 2 h / Heating

3: 97 percent / 1,2-dichloro-ethane / 2.5 h / 80 °C

With potassium permanganate; potassium carbonate; calcium carbonate; In methanol; diethyl ether; water; 1,2-dichloro-ethane; acetone;
DOI:10.1016/S0040-4020(01)86133-0