2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

Base Information

Chemical Name:2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid
CAS No.:1333127-39-1
Molecular Formula:C₁₈H₂₃F₃N₂O₆
Molecular Weight:420.386
Hs Code.:

Synonyms:2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

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Chemical Property of 2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

Chemical Property:

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Technology Process of 2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

There total 1 articles about 2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333127-49-3
4-[tertbutoxycarbonyl(methyl)amino]salicylic acid

: 67680-78-8
N-(3-chloropropyl)-2,2,2-trifluoroacetamide

: 1333127-39-1
2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

Guidance literature:: With potassium carbonate; at 110 ℃; for 1h;

Reference yield:

: 1333127-39-1
2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

: 1333127-40-4
2-[3-(trifluoroacetylamino)-propoxy]-4-(methyl)aminobenzoic acid

Guidance literature:: With hydrogenchloride; water; In ethanol; for 3h;

Reference yield:

: 1333127-39-1
2-[3-(trifluoroacetylamino)-propoxy]-4-[(tert-butoxycarbonyl)(methyl)amino]benzoic acid

: 1333126-97-8
N-(5-chloropyridine-2-yl)-2-{[4-methyl(methylcarbamoyl)-amino]-2-[3-aminopropoxy]phenylcarbonyl}amino-5-methylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / ethanol / 3 h

2: tetrahydrofuran / 78 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 48 h

4: sodium hydroxide; water / ethanol / 2 h

With hydrogenchloride; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; ethanol;