(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

Base Information

Chemical Name:(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal
CAS No.:141873-75-8
Molecular Formula:C₂₈H₃₇NO₆
Molecular Weight:483.605
Hs Code.:

Synonyms:(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

Chemical Property:

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Technology Process of (3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

There total 7 articles about (3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 141873-75-8
(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 60percent NaH / 1.) DMF, -15 deg C, 10 min., 2.) r.t., 2 h

4: 100 percent / acetonitrile / 16 h / Heating

With sodium hydride; In acetonitrile;
DOI:10.1055/s-1992-34166

Reference yield:

: 141873-79-2
(1R,2R)-1,2-O-isopropylidene-1-(2-thiazolyl)-1,2,3-propanetriol

: 141873-75-8
(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 60percent NaH / 1.) DMF, -15 deg C, 10 min., 2.) r.t., 2 h

4: 100 percent / acetonitrile / 16 h / Heating

With sodium hydride; In acetonitrile;
DOI:10.1055/s-1992-34166

Reference yield:

: 141873-73-6
(1R,2R)-3-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-1-(2-thiazolyl)-1,2,3-propanetriol

: 141873-75-8
(3R,4R,5R)-3-benzyl(tert-butoxycarbonyl)amino-6-benzyloxy-4,5-isopropylidenedioxyhexanal

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / Bu₄NF / tetrahydrofuran / 2 h / Ambient temperature

2: 1.) 60percent NaH / 1.) DMF, -15 deg C, 10 min., 2.) r.t., 2 h

5: 100 percent / acetonitrile / 16 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1055/s-1992-34166